Isoctanoic acid was prepared by ultrasonic synthesis

Sep 23,2022


Because isoctanoic acid is more and more widely used, and the traditional production process has some disadvantages such as low rate and long reaction time, so it is urgent to adopt a new synthesis method. In 1991, khurana J. M. used ultrasonic cleaner as ultrasonic source for isoctanoic acid synthesis experiment.

Therefore, it can be inferred that ultrasonic synthesis of isoctanoic acid is a feasible process. It has been shown that ultrasound has a significant stimulatory effect on many reactions. Some reactions are difficult to take place under general conditions or require the presence of catalyst below, while under ultrasonic radiation can be carried out under milder conditions.

The method of synthesizing isoctanoic acid by ultrasonic radiation was used, and 2-ethylhexanol was oxidized by 60% nitric acid at room temperature and pressure with H66005 ultrasonic washing tank as radiation sound source. 25g isooctanol and 30g60%HNO3 were weighed and added into 250ml conical flask in turn. The conical flask was fixed in the center of the ultrasonic cleaning tank, 2 ~ 3cm away from the bottom of the tank. Activate the ultrasonic source for radiation reaction. The reaction time was 1h.

It can be seen that the ultrasonic synthesis method of isoctanoic acid, isoctanoic acid, paint drying agent, degreased naphthenic acid has a significant role in promoting 2-ethylhexanol oxidation reaction, reaction speed, yield and product purity have very good results. Because isoctanoic acid is more and more widely used, and the traditional production process has some disadvantages such as low rate and long reaction time, so it is urgent to adopt a new synthesis method. In 1991, khurana J. M. used ultrasonic cleaner as ultrasonic source for isoctanoic acid synthesis experiment.

Therefore, it can be inferred that ultrasonic synthesis of isoctanoic acid is a feasible process. It has been shown that ultrasound has a significant stimulatory effect on many reactions. Some reactions are difficult to take place under general conditions or require the presence of catalyst below, while under ultrasonic radiation can be carried out under milder conditions.

The method of synthesizing isoctanoic acid by ultrasonic radiation was used, and 2-ethylhexanol was oxidized by 60% nitric acid at room temperature and pressure with H66005 ultrasonic washing tank as radiation sound source. 25g isooctanol and 30g60%HNO3 were weighed and added into 250ml conical flask in turn. The conical flask was fixed in the center of the ultrasonic cleaning tank, 2 ~ 3cm away from the bottom of the tank. Activate the ultrasonic source for radiation reaction. The reaction time was 1h.

It can be seen that the ultrasonic synthesis method of isoctanoic acid, ultrasonic on 2-ethylhexanol oxidation reaction has a significant role in promoting the reaction, reaction speed, yield and product purity are very good results.

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